in further solvent(s) byproducts: PhCCMe; Ar atmosphere, addn. alkene to glyme soln. of Me3SnK (-78°C); addn. water (room temp.), filtration (Ar atmosphere), solvent removal (vac.);
参考文献
Mitchell, T. N.; Reinmann, W.
Organometallics, 1986 , vol. 5, p. 1991 - 1997
in tetrahydrofuran KSnMe3 added to PhSnEt3 in THF, stirred at 50°C for 30 min, hydrolysis with water; org. layer extd. with ether, dried over Na2SO4; products determined by GLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 9 p. 3299 - 3306
in tetrahydrofuran; diethyl ether addn. of Me3SnK in THF/ether to a soln. of 2-bromooctane in THF/ether at 0°C under Ar; quenching after 1 h with a large excess H2O2, extg. (pentane), washing of extracts (H2O), drying (Na2SO4), GLPC;
参考文献
Journal of the American Chemical Society, , vol. 107, # 2 p. 416 - 423
in tetrahydrofuran addn. of Me3SnK in THF to a soln. of 2-bromooctane in THF at 0°Cunder Ar; quenching after 1 h with a large excess H2O2, extg. (pentane), washing of extracts (H2O), drying (Na2SO4), GLPC;
参考文献
Alnajjar, Mikhail S.; Kuivila, Henry G.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 416 - 423
