1-硝基-2-[(三氟甲基)磺酰基]苯合成路线 （共 12 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Journal of Fluorine Chemistry, , vol. 52, # 3 p. 295 - 300
反应条件
potassium fluoride; tetra-phenylphosphonium bromide in dimethyl sulfoxide T=130°C; 0.25 h;
参考文献
Wang, Guangjun; Zhang, Hushan; Zhou, Jing; Ha, Chengyong; Pei, Duanqing; Ding, Ke
Synthesis, 2008 , # 15 art. no. F04408SS, p. 2398 - 2404
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Journal of Fluorine Chemistry, , vol. 52, # 3 p. 295 - 300
反应条件
chromium(VI) oxide
T=100°C;
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
反应条件
methylsulphinylalcohol; nitrogen(IV) oxide; ozone in dichloromethane
T=-10°C; Kyodai-nitration; 2.5 h;
参考文献
Nose, Masatoshi; Suzuki, Hitomi
Synthesis, 2002 , # 8 p. 1065 - 1071
反应条件
1: CrO3 / H2SO4
2: NO2; O3; MeSO2H / CH2Cl2 / 2.5 h / -10 °C
View Scheme
参考文献
Nose, Masatoshi; Suzuki, Hitomi
Synthesis, 2002 , # 8 p. 1065 - 1071
反应条件
dihydrogen peroxide; trifluoroacetic acid
参考文献
Yagupol'skii,L.M.; Boiko,V.N.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, # 1 p. 195 - 198,179 - 182
反应条件
1: aq. H2SO4
2: CF3CO2H, aq. H2O2
View Scheme
参考文献
Yagupol'skii,L.M.; Boiko,V.N.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, # 1 p. 195 - 198,179 - 182
反应条件
1: CrO3, AcOH
2: SO3/H2SO4, NaN3
3: (i) H2SO4, NaNO2, (ii) aq. Na2S2O4, H2SO4
View Scheme
参考文献
Yagupol'skii,L.M.; Gandel'sman,L.Z.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, # 9 p. 2101 - 2108,1992 - 1997
反应条件
1: aq. HNO3, H2SO4
2: CrO3, AcOH
3: SO3/H2SO4, NaN3
4: (i) H2SO4, NaNO2, (ii) aq. Na2S2O4, H2SO4
View Scheme
参考文献
Yagupol'skii,L.M.; Gandel'sman,L.Z.
J. Gen. Chem. USSR (Engl. Transl.), 1967 , vol. 37, # 9 p. 2101 - 2108,1992 - 1997
