2,2’,3,5’,6-戊氯联苯合成路线 (共 4 条)
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tripotassium phosphate monohydrate; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Joshi; Vyas; Duffel; Parkin; Lehmler
Synthesis, 2011 , # 7 p. 1045 - 1054
反应条件
Cu bronze T=230°C; Ullmann reaction; 168 h; Inert atmosphere;
参考文献
Joshi; Vyas; Duffel; Parkin; Lehmler
Synthesis, 2011 , # 7 p. 1045 - 1054
反应条件
poly(sodium styrenesulfonate-co-2-vinylnaphthalene) in water 24 h; Irradiationvar. time, solvent and concentration of HCB, several additional products; Product distributionMechanism;
参考文献
Nowakowska; Sustar; Guillet
Journal of the American Chemical Society, 1991 , vol. 113, # 1 p. 253 - 258
反应条件
sodium acetate; HNO2 Arylation; Gomberg-Bachman reaction;
参考文献
Bolgar; et al.
Chemosphere, 1995 , vol. 31, # 2 p. 2687 - 2705