1,1,1-三氟-2-戊酮合成路线 (共 13 条)
反应条件
baker's yeast in water
T=35 - 37°C; 240 h;
参考文献
Kitazume, Tomoya; Ishikawa, Nobuo
Chemistry Letters, 1984 , p. 587 - 590
反应条件
baker's yeast in water
T=35 - 37°C; 240 h;
参考文献
Kitazume, Tomoya; Ishikawa, Nobuo
Chemistry Letters, 1984 , p. 587 - 590
反应条件
anhydrous butyl ether
参考文献
Dishart; Levine
Journal of the American Chemical Society, 1956 , vol. 78, p. 2268
反应条件
zinc in pyridine
T=20°C; P=2250.2 - 3000.2 Torr; 2.5 h; other anhydrides; other perfluoroalkyl iodide;
参考文献
Francese, C.; Tordeux, M.; Wakselman, C.
Tetrahedron Letters, 1988 , vol. 29, # 9 p. 1029 - 1030
反应条件
magnesium bromide in anhydrous butyl ether
参考文献
Gassen, Karl-Rudolf; Kirmse, Wolfgang
Chemische Berichte, 1986 , vol. 119, # 7 p. 2233 - 2248
反应条件
diethyl ether
und Hydrolyse mit 20prozent ig. wss. Schwefelsaeure;
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 917
反应条件
diethyl ether; sodium methylate
参考文献
Barkley; Levine
Journal of the American Chemical Society, 1953 , vol. 75, p. 2059,2061
反应条件
in water
T=35 - 36°C; 240 h; backer's yeast in Na2PO4, KH2PO4 buffer (pH = 7.3); Yields of byproduct given;
参考文献
Kitazume,T.; Ishikawa,N.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 431
参考文献
Burdon,J.; McLoughlin,V.C.R.
Tetrahedron, 1964 , vol. 20, p. 2162 - 2166
反应条件
diethyl ether; trifluoro magnesium iodide
参考文献
Haszeldine
Journal of the Chemical Society, 1954 , p. 1273,1278