2,2′-双(溴甲基)-1,1′-联苯合成路线 （共 52 条）
反应条件
magnesium in diethyl ether Heating;
参考文献
Cosmo, Robert; Sternhell, Sever
Australian Journal of Chemistry, 1987 , vol. 40, # 1 p. 35 - 47
反应条件
1: hydrazinecarboxylic acid tert-butyl ester With n-butyllithium in tetrahydrofuran; hexane T=-78 - -45°C; 0.25 h; Inert atmosphere; 2: 2,2'-bis(bromomethyl)-1,1'-biphenyl in tetrahydrofuran; hexane T=-45°C; 1 h; Inert atmosphere;
参考文献
Organometallics, , vol. 33, # 1 p. 188 - 193
反应条件
1: N1-Boc-N2-phenyl-hydrazine With n-butyllithium in tetrahydrofuran; hexane T=-78 - -45°C; 0.25 h; Inert atmosphere; 2: 2,2'-bis(bromomethyl)-1,1'-biphenyl in tetrahydrofuran; hexane T=-45°C; 1 h; Inert atmosphere;
参考文献
Organometallics, , vol. 33, # 1 p. 188 - 193
反应条件
1: N1-Boc-N2-phenyl-hydrazine With n-butyllithium in tetrahydrofuran; hexane T=-78 - -45°C; 0.25 h; Inert atmosphere; 2: 2,2'-bis(bromomethyl)-1,1'-biphenyl in tetrahydrofuran; hexane T=-45°C; 24 h; Inert atmosphere;
参考文献
Organometallics, , vol. 33, # 1 p. 188 - 193
反应条件
T=550 - 825°C; P=1 Torr; flow-vacuum pyrolysis; Further byproducts given;
参考文献
Istrati, Daniela; Marton, George; Draghici, Constantin; Grigore, Adriana; Banciu, Mircea D.
Revue Roumaine de Chimie, 2005 , vol. 50, # 7-8 p. 719 - 724
反应条件
diethyl ether; magnesium
参考文献
Hall et al.
Journal of the Chemical Society, 1950 , p. 711
参考文献
Hall et al.
Journal of the Chemical Society, 1950 , p. 711
反应条件
lithium 1.) NH3/THF, -60 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Krummel, Guenter; Muellen, Klaus
Tetrahedron Letters, 1988 , vol. 29, # 23 p. 2809 - 2812
参考文献
Schroeter; Mueller; Huang
Chemische Berichte, 1929 , vol. 62, p. 649
反应条件
Behandeln des Reaktionsgemisches mit wss. HCl;
参考文献
Hall et al.
Journal of the Chemical Society, 1950 , p. 711
