2-三氟甲基-1,1,1,3,3,3-六氟丙烷合成路线 （共 44 条）
反应条件
potassium fluoride in acetonitrile
1) 0 deg C, 1 hour 2) 20 deg C, 11-12 h;
参考文献
Doroginskii, V. A.; Kolomiets, A. F.; Sokol'skii, G. A.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 672 - 675
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 742 - 746
反应条件
triethylsilane; 2,3,4,5,6-pentafluorostyrene in benzene-d6
T=24.9°C; 22 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dolbier Jr., William R.; Li, An-Rong
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 1 p. 79 - 82
反应条件
in further solvent(s)
95°C, 1 h, in SbF5;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
diiron nonacarbonyl in hexane
参考文献
Nesmeyanov,A.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1973 , vol. 43, # 9 p. 2007 - 2012,1993 - 1997
反应条件
moisture; Copper(I) trifluoromethanethiolate in acetonitrile
1.) -78 deg C, 2 h, 2.) from 55 deg C to 60 deg C, 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Munavalli, S.; Lewis, E. O.; Muller, A. J.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.
Journal of Fluorine Chemistry, 1993 , vol. 63, # 3 p. 253 - 264
反应条件
cesium fluoride
T=80°C; 40 h;
参考文献
Postovoi, S. A.; Zeifman, Yu. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 197 - 198
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 209 - 211
反应条件
triethylamine; N,N-dimethyl-formamide
参考文献
Cheburkov,Yu.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1970 , # 10 p. 2135 - 2138
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1970 , # 10 p. 2272 - 2275
反应条件
2,3,4,5,6-pentafluorobenzene; SbF5
参考文献
Belen'kii,G.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, # 6 p. 1191 - 1195
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, # 6 p. 1183 - 1187
参考文献
Del'tsova, D. P.; Safronova, Z. V.; Gambaryan, N. P.; Knunyants, N. L.
Doklady Chemistry, 1982 , vol. 267, p. 437 - 440
Dokl. Akad. Nauk SSSR Ser. Khim., 1982 , vol. 267, # 4 p. 856 - 859
反应条件
water in acetone
T=20°C; 168 h; Product distribution;
参考文献
Knunyants, I. L.; Zeifman, Yu. V.; Lantseva, L. T.
Doklady Chemistry, 1980 , vol. 254, p. 417 - 420
Dokl. Akad. Nauk SSSR Ser. Khim., 1980 , vol. 254, # 1 p. 117 - 120
