1,3-双[(三甲基硅基)乙炔基]苯合成路线 （共 6 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine in tetrahydrofuran T=70°C; Sonogashira coupling; 1 h; Inert atmosphere;
参考文献
Lee, Semin; Hua, Yuran; Park, Hyunsoo; Flood, Amar H.
Organic Letters, 2010 , vol. 12, # 9 p. 2100 - 2102
反应条件
bis(benzonitrile)palladium(II) dichloride; meta-dibromobenzene; copper diacetate; diisopropylamine; triphenylphosphine 3 h; Heating;
参考文献
Neenan, Thomas X.; Whitesides, George M.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2489 - 2496
反应条件
bis(benzonitrile)palladium(II) dichloride; copper diacetate; diisopropylamine; triphenylphosphine 3 h; Heating;
参考文献
Neenan, Thomas X.; Whitesides, George M.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2489 - 2496
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine in tetrahydrofuran T=65°C; Sonogashira Cross-Coupling; 24 h;
参考文献
Fu, Tsung-Hao; Li, Yan; Thaker, Hitesh D.; Scott, Richard W.; Tew, Gregory N.
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 9 p. 841 - 845
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diisopropylamine in toluene Sonogashira coupling; Inert atmosphereHeating;
参考文献
Yang, Xin; Matsuo, Daisuke; Suzuma, Yoshinori; Fang, Jing-Kun; Xu, Feng; Orita, Akihiro; Otera, Junzo; Kajiyama, Shingo; Koumura, Nagatoshi; Hara, Kohjiro
Synlett, 2011 , # 16 art. no. U04611ST, p. 2402 - 2406
反应条件
potassium hydroxide; water in methanol 0.333333 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 53, # 11 p. 2489 - 2496
