3-苯基环戊-2-烯-1-酮合成路线 （共 62 条）
反应条件
tert.-butylhydroperoxide; potassium carbonate; palladium on activated charcoal in dichloromethane
T=0 - 23°C; 15 h;
参考文献
Yu, Jin-Quan; Corey
Organic Letters, 2002 , vol. 4, # 16 p. 2727 - 2730
反应条件
sodium hydroxide in water
4 h; Reflux;
参考文献
Peloquin, Andrew J.; Stone, Rebecca L.; Avila, Sarah E.; Rudico, Erlyn R.; Horn, Christopher B.; Gardner, Kim A.; Ball, David W.; Johnson, Jane E. B.; Iacono, Scott T.; Balaich, Gary J.
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 6371 - 6376
反应条件
sodium acetate; antimony trichloride; palladium diacetate in acetic acid
T=25°C; 24 h;
参考文献
Cho, Chan Sik; Motofusa, Shin-ichi; Ohe, Kouichi; Uemura, Sakae; Shim, Sang Chul
Journal of Organic Chemistry, 1995 , vol. 60, # 4 p. 883 - 888
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide
T=55°C; 0.5 h;
参考文献
Shibuya, Masatoshi; Ito, Shinichiro; Takahashi, Michiyasu; Iwabuchi, Yoshiharu
Organic Letters, 2004 , vol. 6, # 23 p. 4303 - 4306
反应条件
1: With (x)BF4*C9H14NO(1+) in dichloromethane
T=-78°C; 1 h;
2: With sodium hydrogencarbonate in dichloromethane; water
T=20°C;
参考文献
Hayashi, Masaki; Shibuya, Masatoshi; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 1 p. 154 - 157
反应条件
in tetrahydrofuran; diethyl ether; cyclohexane
T=20°C; 16 h;
参考文献
Jurkauskas, Valdas; Buchwald, Stephen L.
Journal of the American Chemical Society, 2002 , vol. 124, # 12 p. 2892 - 2893
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Jurkauskas, Valdas; Sadighi, Joseph P.; Buchwald, Stephen L.
Organic Letters, 2003 , vol. 5, # 14 p. 2417 - 2420
反应条件
tetrabutyl ammonium fluoride; antimony trichloride; acetic acid; palladium diacetate in acetonitrile
T=60°C; 28 h;
参考文献
Denmark, Scott E.; Amishiro, Nobuyoshi
Journal of Organic Chemistry, 2003 , vol. 68, # 18 p. 6997 - 7003
反应条件
potassium carbonate; C40H45O2N2P2PdCl2 in toluene
T=140°C; Heck coupling reaction; 4 h;
参考文献
Krishna, Thatavarathy Rama; Jayaraman, Narayanaswamy
Tetrahedron, 2004 , vol. 60, # 45 p. 10325 - 10334
反应条件
[Cp*RhCl2]2 in toluene
T=80°C; P=38002.6 Torr; 5 h; Autoclave;
参考文献
Brancour, Celia; Fukuyama, Takahide; Ohta, Yuko; Ryu, Ilhyong; Dhimane, Anne-Lise; Fensterbank, Louis; Malacria, Max
Chemical Communications, 2010 , vol. 46, # 30 p. 5470 - 5472
反应条件
[Pd(1,2-bis(diphenylphosphanyl)ethane)(PhCN)2](SbF6)2; potassium carbonate in tetrahydrofuran
T=20°C; 23 h;
参考文献
Nishikata, Takashi; Yamamoto, Yasunori; Miyaura, Norio
Angewandte Chemie - International Edition, 2003 , vol. 42, # 24 p. 2768 - 2770
