4-甲基硫代-ortho-甲酚合成路线 (共 8 条)
反应条件
tetra-n-butylammonium tetrafluoroborate in dichloromethane
参考文献
Do, Quang Tho; Elothmani, Driss; Le Guillanton, Georges
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4657 - 4658
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
反应条件
1: 26 percent / ClSO2OH / diethyl ether / 12 h / Ambient temperature
2: 94 percent / Heating
View Scheme
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
反应条件
aluminium trichloride in tetrachloromethane
Friedel-Crafts reaction; 1 h; Heating;
参考文献
Oyaizu, Kenichi; Mikami, Takefumi; Mitsuhashi, Fumio; Tsuchida, Eishun
Macromolecules, 2002 , vol. 35, # 1 p. 67 - 78
反应条件
in tetrachloromethane
参考文献
Farah,B.S.; Gilbert,E.E.
Journal of Organic Chemistry, 1963 , vol. 28, p. 2807 - 2809
参考文献
Kouge; Koizumi; Okai; Kato
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 7 p. 2409 - 2418
反应条件
potassium hydroxide in methanol
16 h; Heating;
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
反应条件
in acetone
in presence of (C2H5)3N, 20°C, 1 h, under N2 atmosphere;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.4, page 152 - 186