1-苯基-2,3,4,9-四氢-1H-beta-咔啉合成路线 (共 50 条)
反应条件
1-propanephosphonic acid cyclic anhydride in ethyl acetate T=110°C; 0.166667 h; Microwave irradiationSealed tube; TimeTemperature;
参考文献
Desroses, Matthieu; Koolmeister, Tobias; Jacques, Sylvain; Llona-Minguez, Sabin; Jacques-Cordonnier, Marie-Caroline; Cazares-Koerner, Armando; Helleday, Thomas; Scobie, Martin
Tetrahedron Letters, 2013 , vol. 54, # 27 p. 3554 - 3557
反应条件
sodium tetrahydroborate T=20°C; 12 h;
参考文献
Espinoza-Moraga, Marlene; Caballero, Julio; Gaube, Friedemann; Winckler, Thomas; Santos, Leonardo S.
Chemical Biology and Drug Design, 2012 , vol. 79, # 4 p. 594 - 599
反应条件
trifluoroacetic acid in ethanol; chloroform T=20 - 60°C; 22 h;
参考文献
Dong, Jing; Shi, Xiao-Xin; Yan, Jing-Jing; Xing, Jing; Zhang, Qiang; Xiao, Sen
European Journal of Organic Chemistry, 2010 , # 36 p. 6987 - 6992
反应条件
chloro-trimethyl-silane; ytterbium(III) triflate in tetrahydrofuran; dichloromethane T=20°C; Pictet-Spengler reaction; 5 h;
参考文献
Tsuji, Riichiro; Yamanaka, Masamichi; Nishida, Atsushi; Nakagawa, Masako
Chemistry Letters, 2002 , # 4 p. 428 - 429
反应条件
1: molecular sives 4A / CH2Cl2 / Ambient temperature 2: 68 percent / pyridine / CH2Cl2 / Ambient temperature 3: 71 percent / Zn / acetic acid View Scheme
参考文献
Kawate, Tomohiko; Nakagawa, Masako; Ogata, Koreharu; Hino, Tohru
Heterocycles, 1992 , vol. 33, # 2 p. 801 - 811
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran; diethyl ether T=-23°C; 3 h;
参考文献
Nakagawa, Masako; Kawate, Tomohiko; Yamazaki, Hitoshi; Hino, Thoru
Journal of the Chemical Society, Chemical Communications, 1990 , # 14 p. 991 - 992
反应条件
hydrogenchloride in acetonitrile 0.2 h; Ambient temperature;
参考文献
Singh, Harjit; Sarin, Rakesh
Journal of Chemical Research, Miniprint, 1988 , # 10 p. 2623 - 2640
反应条件
hydrogenchloride in acetonitrile 0.2 h; Ambient temperature;
参考文献
Singh, Harjit; Sarin, Rakesh
Journal of Chemical Research, Miniprint, 1988 , # 10 p. 2623 - 2640
反应条件
trifluoroacetic acid in acetonitrile 12 h; Heating;
参考文献
Singh, Harjit; Sarin, Rakesh
Heterocycles, 1985 , vol. 23, # 1 p. 107 - 110
反应条件
trifluoroacetic acid in acetonitrile 9 h; Heating;
参考文献
Singh, Harjit; Sarin, Rakesh
Journal of Chemical Research, Miniprint, 1988 , # 10 p. 2623 - 2640