(S)-2-苯基-1-丙醇合成路线 （共 88 条）
反应条件
Jone's reagent in acetone T=0°C; 8 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Nandanan; Jayachandran; Phukan, Prodeep; Pais, Godwin C. G.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 12 p. 1221 - 1227
反应条件
Jone's reagent in acetone T=0°C; 8 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Nandanan; Jayachandran; Phukan, Prodeep; Pais, Godwin C. G.; Sudalai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 12 p. 1221 - 1227
反应条件
Dess-Martin periodane in dichloromethane 1.66667 h; Inert atmosphere;
参考文献
Schueler, Peter; Fischer, Sebastiann.; Marsch, Michael; Oberthuer, Markus
Synthesis (Germany), 2013 , vol. 45, # 1 art. no. SS-2012-E0759-FA, p. 27 - 39
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide Title compound not separated from byproducts.;
参考文献
Hashimoto, Toru; Ito, Jun-ichi; Nishiyama, Hisao
Tetrahedron, 2008 , vol. 64, # 40 p. 9408 - 9412
反应条件
methane; oxygen in gaseous matrix T=25°C; Irradiationother temperatures; Product distributionKineticsMechanism;
参考文献
Speranza, Maurizio; Filippi, Antonello
Chemistry - A European Journal, 1999 , vol. 5, # 3 p. 834 - 844
反应条件
1: pyridine 2: NaN3 / dimethylsulfoxide / 20 h / 80 °C 3: LiAlH4 / diethyl ether View Scheme
参考文献
Kirmse, Wolfgang; Guenther, Bernd-Rainer; Loosen, Karin
Chemische Berichte, 1980 , vol. 113, # 6 p. 2140 - 2153
反应条件
1: pyridine 2: NaN3 / dimethylsulfoxide / 20 h / 80 °C 3: LiAlH4 / diethyl ether View Scheme
参考文献
Kirmse, Wolfgang; Guenther, Bernd-Rainer; Loosen, Karin
Chemische Berichte, 1980 , vol. 113, # 6 p. 2140 - 2153
反应条件
1.1: 85 percent / Ph3P; 1H-imidazole; I2 / diethyl ether; acetonitrile / 3 h / 20 °C
2.1: BuLi; diisopropylamine / hexane; tetrahydrofuran; hexamethylphosphoric acid triamide / 0.5 h / -25 - 0 °C
2.2: 54 percent / HMPA / tetrahydrofuran; hexane / 1 h / 20 °C
3.1: 76 percent / KOH / methanol / 0.17 h / 0 °C
4.1: 57 percent / Rh2(OAc)4 / CH2Cl2 / 3 h / 0 °C
5.1: 68 percent / dimethylsulfoxide; H2O / 24 h / Heating
View Scheme
参考文献
Mueller, Paul; Bolea, Christelle
Helvetica Chimica Acta, 2002 , vol. 85, # 2 p. 483 - 494
