1-(4-硝基苯基)-2-苯乙酮合成路线 (共 18 条)
反应条件
scandium tris(trifluoromethanesulfonate) in toluene
T=-78°C; 0.166667 h; Inert atmosphere;
参考文献
Wommack, Andrew J.; Moebius, David C.; Travis, Austin L.; Kingsbury, Jason S.
Organic Letters, 2009 , vol. 11, # 15 p. 3202 - 3205
反应条件
[CpFe(CO)2(THF)][BF4] in dichloromethane
T=20°C; Cycloaddition; insertion; 12.5 h;
参考文献
Mahmood, Syed J.; Saha, Anjan K.; Mahmun Hossain
Tetrahedron, 1998 , vol. 54, # 3-4 p. 349 - 358
反应条件
in tetrahydrofuran; water
T=50°C; 48 h;
参考文献
Aggarwal, Varinder K.; De Vicente, Javier; Pelotier, Beatrice; Holmes, Ian P.; Bonnert, Roger V.
Tetrahedron Letters, 2000 , vol. 41, # 52 p. 10327 - 10331
反应条件
sodium methylate in methanol; N,N-dimethyl-formamide
1 h; Ambient temperature;
参考文献
Patonay, Tamas; Hegedues, Laszlo; Patonay-Peli, Erzsebet
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 1 p. 145 - 151
反应条件
zinc(II) iodide in diethyl ether
2 h; Ambient temperature;
参考文献
Bartnik, R.; Mloston, G.
Acta Chimica Academiae Scientiarum Hungaricae, 1981 , vol. 106, # 4 p. 309 - 312
反应条件
sulfuric acid in water
0.333333 h; Heating; Yield given. Yields of byproduct given;
参考文献
Bansal, R K; Sharma, V K
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 5 p. 482 - 485
反应条件
2: N2O4 / CCl4
3: Fe, aq. HCl / ethanol / Heating
View Scheme
参考文献
Colau,R.; Viel,C.
Bulletin de la Societe Chimique de France, 1979 , vol. <II>, p. 362 - 365
反应条件
hydrogenchloride; iron in ethanol
Heating;
参考文献
Colau,R.; Viel,C.
Bulletin de la Societe Chimique de France, 1979 , vol. <II>, p. 362 - 365
反应条件
1: 54 percent / pyridine / CHCl3 / 96 h
2: 50 percent / NaOMe / dimethylformamide; methanol / 1 h / Ambient temperature
View Scheme
参考文献
Patonay, Tamas; Hegedues, Laszlo; Patonay-Peli, Erzsebet
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 1 p. 145 - 151
反应条件
1: N2O4 / CCl4
2: Fe, aq. HCl / ethanol / Heating
View Scheme
参考文献
Colau,R.; Viel,C.
Bulletin de la Societe Chimique de France, 1979 , vol. <II>, p. 362 - 365