1,1,1-三甲基-N-苯基哌啶合成路线 （共 76 条）
反应条件
1: HN(SiMe3)(Ph) With n-butyl-magnesium bromide in anhydrous butyl ether T=0 - 100°C; 1 h; Inert atmosphere; 2: 1-Bromonaphthalene With lithium bromide; iron(II) chloride in anhydrous butyl ether T=140°C; 24 h; Inert atmosphere;
参考文献
Hatakeyama, Takuji; Imayoshi, Ryuji; Yoshimoto, Yuya; Ghorai, Sujit K.; Jin, Masayoshi; Takaya, Hikaru; Norisuye, Kazuhiro; Sohrin, Yoshiki; Nakamura, Masaharu
Journal of the American Chemical Society, 2012 , vol. 134, # 50 p. 20262 - 20265
参考文献
Kreschkow et al.
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1959 , vol. 32, p. 369,370;engl.Ausg.S.384,385
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=20°C; 0.0833333 h;
参考文献
Iida, Akira; Horii, Atsushi; Misaki, Tomonori; Tanabe, Yoo
Synthesis, 2005 , # 16 art. no. F06305SS, p. 2677 - 2682
反应条件
n-butyllithium in diethyl ether
参考文献
Chandrasekhar, Vadapalli; Boomishankar, Ramamoorthy; Azhakar, Ramachandran; Gopal, Kandasamy; Steiner, Alexander; Zacchini, Stefano
European Journal of Inorganic Chemistry, 2005 , # 10 p. 1880 - 1885
反应条件
lithium perchlorate in diethyl ether 0.5 h;
参考文献
Saidi, Mohammad R; Azizi, Najmoddin; Zali-Boinee, Hasan
Tetrahedron, 2001 , vol. 57, # 31 p. 6829 - 6832
反应条件
1: N-bromosuccinimide / CCl4 / 24 h / -20 °C 2: CH3OH / 0.02 h View Scheme
参考文献
Synthesis, , # 4 p. 263 - 264
参考文献
Anderson, H. H.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5802 - 5803
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Gmelin Handbook: Si: MVol.C, 111, page 310 - 313
参考文献
Anderson, H. H.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5802 - 5803
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 111, page 310 - 313
参考文献
Kreschkow et al.
Zhurnal Obshchei Khimii, 1958 , vol. 28, p. 2112;engl.Ausg.S.2150
反应条件
in decane addn. of a soln. of Me3SiNHC6H5 in decane to 2,4,6-tri-t-butylphenyl difluoroborane and vigorously refluxing for 3-5 d under N2; distilling off the excess of amine and fractional distn. of the phenylaminoborane from the residue, elem. anal.;
参考文献
Geschwentner, M.; Elter, G.; Meller, A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1993 , vol. 619, p. 1474 - 1478
