sodium in neat (no solvent)
stoich. amt. of sodium (2 mol for 1 mol of ditin oxide), 120°C, 48 h; unreacted n-Pen6Sn2O was removed by filtration in pentane through a short SiO2 column, n-Pen4Sn was removed by distn.;
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.8, page 113 - 114
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.8, page 113 - 114