1,1,2,2,3,3,4,4,5,5-十氟环戊烷合成路线 (共 22 条)
反应条件
T=1250°C; P=500 Torr; Pyrolysis;
参考文献
Steunenberg; Cady
Journal of the American Chemical Society, 1952 , vol. 74, p. 4165
反应条件
T=1250°C; P=500 Torr; Pyrolysis;
参考文献
Steunenberg; Cady
Journal of the American Chemical Society, 1952 , vol. 74, p. 4165
反应条件
Irradiation; Rate constant;
参考文献
Journal of Physical Chemistry, , vol. 92, # 1 p. 102 - 106
反应条件
cobalt(III) fluoride
T=200 - 300°C;
参考文献
Burford et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 319,328
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Fowler et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 292,297
反应条件
nitrogen; copper; fluorine
T=90°C;
参考文献
Fukuhara; Bigelow
Journal of the American Chemical Society, 1941 , vol. 63, p. 2793
反应条件
carbon in neat (no solvent)
further products;;
参考文献
Simons; Block
Journal of the American Chemical Society, 1937 , vol. 59, p. 1407
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Simons, J. H.; Block, L. P.
Journal of the American Chemical Society, 1939 , vol. 61, p. 2962 - 2966
反应条件
fluorine
T=-30 - 10°C; Irradiationsteady-state flow process; the hydrocarbon vapor is condensed onto a NaF preaerosol and then subjected to attack by an excess of elemental F in He at first in the dark, then under UV irradiation; Further byproducts given. Yields of byproduct given;
参考文献
Adcock, James L.; Evans, William D.
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2719 - 2723
反应条件
hydrogen fluoride
T=5 - 6°C; 7.45 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.5 - 9.0 V; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 7.31667 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.1 - 8.0 V; Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 7.1 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.7 - 8.1 V; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123