4,4'-联苯二甲基二甲醚合成路线 (共 3 条)
反应条件
zinc; 5-trimethylsilyl-2,2'-bipyridine; niobium bromide in 1-methyl-pyrrolidin-2-one T=20 - 70°C; Inert atmosphere;
参考文献
EP2172470 A1, ;
Page/Page column 43 ;
反应条件
mordenite SiO2/Al2O3 90 in cyclohexane T=120°C; 4 h; Product distribution / selectivity;
参考文献
WO2006/89900 A1, ;
Page/Page column 15-16 ;
反应条件
Sodium bromate; acetic acid T=90°C; 1.5 h; Product distribution / selectivity;
参考文献
IHARA CHEMICAL INDUSTRY CO., LTD.
Patent: EP1661877 A1, 2006 ;
Location in patent: Page/Page column 14 ;