1,1,1,2,2,3,3-七氟代-3-甲氧基丙烷合成路线 (共 7 条)
反应条件
cobalt(III) fluoride T=-196 - 20°C; Fluorination; 0.5 h;
参考文献
Synlett, , # 3 p. 343 - 344
反应条件
cesium fluoride in N,N-dimethyl-formamide T=20°C; 3 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 9.1. p. 1870 - 1876
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2057 - 2063
反应条件
bis [2-(2-methoxyethoxy)ethyl] ether; cesium fluoride T=100°C; 48 h;
参考文献
Journal of Fluorine Chemistry, , vol. 126, # 11-12 p. 1578 - 1586
反应条件
NAF in acetonitrile-D3
参考文献
Journal of Fluorine Chemistry, , vol. 119, # 1 p. 3 - 8
反应条件
1: pentafluoropropionyl fluoride With triethylamine tris(hydrogen fluoride); triethylamine 2: dimethyl sulfate With triisooctyl amine T=45 - 47°C; 5.5 h; 3: ethanol T=-78°C;
参考文献
Journal of Fluorine Chemistry, , vol. 118, # 1-2 p. 123 - 126
反应条件
in acetonitrile-D3 T=20°C; 0.5 h; Product distribution; Further Variations:Temperaturestime;
参考文献
Journal of Fluorine Chemistry, , vol. 119, # 1 p. 3 - 8
反应条件
hydroxide T=24.85°C; Kinetics; Further Variations:Temperatures;
参考文献
Chen; Kutsuna; Tokuhashi; Sekiya
Chemical Physics Letters, 2004 , vol. 400, # 4-6 p. 563 - 568