乙酸 2-(1-甲基乙亚基)酰肼合成路线 （共 11 条）
反应条件
1: With triethylamine; phosphorus trichoride in dichloromethane T=20°C; 2: With triethylamine in benzene
参考文献
Guo, Xiangyun; Feng, Li; Wang, Quanrui; Li, Zhiming; Tao, Fenggang
Journal of Heterocyclic Chemistry, 2006 , vol. 43, # 2 p. 353 - 359
反应条件
in cyclohexane
T=55°C; 16 h;
参考文献
Genentech, Inc.
Patent: US2012/245144 A1, 2012 ;
Location in patent: Page/Page column 125 ;
反应条件
in benzene
T=0 - 7°C; 72 h;
参考文献
Khusainova, Narkis G.; Mostovaya, Olga A.; Azancheev, Nail M.; Litvinov, Igor A.; Krivolapov, Dmitry B.; Cherkasov, Rafael A.
Mendeleev Communications, 2004 , vol. 14, # 5 p. 212 - 214
反应条件
1: T=0°C;
2: T=5 - 7°C; 168000 h; Further stages. Title compound not separated from byproducts.;
参考文献
Khusainova; Mostovaya; Cherkasov
Russian Journal of General Chemistry, 2006 , vol. 76, # 3 p. 495 - 496
反应条件
2-acetyl-3-ethoxy-5-methyl-3,4-dihydro-2H-[1,2,3]diazaphosphole in benzene
8 h; Heatingother 1,2,3-diazaphospholes; Mechanism;
参考文献
Chen, Ruyu; Cai, Baozhong
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 57, # 1/2 p. 83 - 85
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
反应条件
1: Pb(OAc)4
2: benzene-d6 / Heating
View Scheme
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
反应条件
1: Pb(OAc)4
2: benzene-d6 / Heating
View Scheme
参考文献
Keus, Diane; Kaminski, Maciej; Warkentin, John
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 343 - 347
