2-[(二乙氨基)-甲基]-环己酮盐酸盐合成路线 （共 8 条）
反应条件
trimethylsilyl iodide in acetonitrile
T=20°C; 1 h;
参考文献
Kozyukov, V. P.; Kozyukov, Vik. P.; Mironov, V. F.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 2 p. 467 - 468,414 - 415
反应条件
in methanol
T=22°C; P=6750540 Torr; 48 h;
参考文献
Matsumoto, Kiyoshi
Angewandte Chemie, 1982 , vol. 94, # 12 p. 937
反应条件
α-cyclohexylcyclohexanemethanamine; trimethylsilyl iodide in acetonitrile
13 h; Ambient temperature;
参考文献
Hosomi, Akira; Iijima, Susumu; Sakurai, Hideki
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 547 - 550
反应条件
1: triethylamine, sodium iodide / acetonitrile / 0.25 h / Ambient temperature
2: acetonitrile / 0 °C
View Scheme
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668
反应条件
1: methyltrichlorosilane / acetonitrile / 0.08 h / 10 °C
2: acetonitrile / 0 °C
View Scheme
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668
反应条件
in acetonitrile
T=0°C; Yield given;
参考文献
Rochin, C.; Babot, O.; Dunogues, J.; Duboudin, F.
Synthesis, 1986 , # 8 p. 667 - 668
反应条件
in tetrahydrofuran
5 h; Heating;
参考文献
Miyano, Sotaro; Mori, Akira; Hokari, Hiroshi; Ohta, Katsuaki; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1331 - 1332
参考文献
Mannich; Hoenig
Archiv der Pharmazie (Weinheim, Germany), 1927 , p. 601
