3,4-二氢-6-甲基-2H-吡喃-2-酮合成路线 （共 30 条）
参考文献
Schulte et al.
Archiv der Pharmazie (Weinheim, Germany), 1958 , vol. 291, p. 227,236
反应条件
sodium methylate in benzene
参考文献
Shusherina,N.P. et al.
Journal of Organic Chemistry USSR (English Translation), 1966 , vol. 2, p. 1771 - 1773
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 1801 - 1804
反应条件
bromine; sodium hydrogencarbonate 1.) CCl4, O deg C; 2.) 25 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Mandal, A.K.; Jawalkar, D.G.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2364 - 2369
反应条件
aluminum oxide; nickel T=180 - 200°C; Hydrogenation;
参考文献
Zhurnal Obshchei Khimii, , vol. 26, p. 750,574; engl. Ausg. S. 861, 864
反应条件
in diethyl ether T=-78°C; 16 h; Inert atmosphere;
参考文献
Simon, Robert C.; Grischek, Barbara; Zepeck, Ferdinand; Steinreiber, Andreas; Belaj, Ferdinand; Kroutil, Wolfgang
Angewandte Chemie - International Edition, 2012 , vol. 51, # 27 p. 6713 - 6716
参考文献
Justus Liebigs Annalen der Chemie, , vol. 294, p. 332
参考文献
Justus Liebigs Annalen der Chemie, , vol. 294, p. 332
参考文献
Schuscherina et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 750,574; engl. Ausg. S. 861, 864
Full Text Show Details
Jacobs; Scott
Journal of Biological Chemistry, 1930 , vol. 87, p. 610
反应条件
sulfuric acid in N,N-dimethyl acetamide
T=100°C; Fischer indole reaction; 2 h;
参考文献
Campos, Kevin R.; Woo, Jacqueline C. S.; Lee, Sandra; Tillyer, Richard D.
Organic Letters, 2004 , vol. 6, # 1 p. 79 - 82
反应条件
lithium diisopropyl amide
1.) THF, -78 deg C, 0.5 h, 2.) THF, a) -78 deg C, 4 h, b) 25 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Belmont, Daniel T.; Paquette, Leo A.
Journal of Organic Chemistry, 1985 , vol. 50, # 21 p. 4102 - 4107
