苯并(a)萘并(2,3-h)吖啶-5,8,13(14H)-三酮合成路线 （共 12 条）
反应条件
nitrobenzene; acetyl chloride
T=100 - 120°C;
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
参考文献
BASF
Patent: DE248170 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 666
反应条件
naphthalene; oxalic acid; nitrobenzene
参考文献
I. G. Farbenind.
Patent: DE450921 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 15, p. 699
反应条件
boric acid; sodium carbonate; nitrobenzene
参考文献
ICI
Patent: US2689247 , 1951 ;
反应条件
1: nitrobenzene; iodine; sulfuryl chloride
2: nitrobenzene; bromine / 160 - 170 °C
4: sodium bi chromate; glacial acetic acid
5: potassium acetate; copper acetate; amyl alcohol
6: nitrobenzene; acetic acid anhydride / 100 - 120 °C
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: nitrobenzene; bromine / 160 - 170 °C
3: sodium bi chromate; glacial acetic acid
4: potassium acetate; copper acetate; amyl alcohol
5: nitrobenzene; acetic acid anhydride / 100 - 120 °C
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: potassium acetate; copper acetate; amyl alcohol
2: nitrobenzene; acetic acid anhydride / 100 - 120 °C
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: hydrochloric acid; sodium chlorate
2: nitrobenzene; bromine / 160 - 170 °C
4: sodium bi chromate; glacial acetic acid
5: potassium acetate; copper acetate; amyl alcohol
6: nitrobenzene; acetic acid anhydride / 100 - 120 °C
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
1: sodium bi chromate; glacial acetic acid
2: potassium acetate; copper acetate; amyl alcohol
3: nitrobenzene; acetic acid anhydride / 100 - 120 °C
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
反应条件
2: sodium bi chromate; glacial acetic acid
3: potassium acetate; copper acetate; amyl alcohol
4: nitrobenzene; acetic acid anhydride / 100 - 120 °C
View Scheme
参考文献
Ullmann; Bincer
Chemische Berichte, 1916 , vol. 49, p. 740
