N-(氧代亚甲基)-beta-丙氨酰氯合成路线 （共 8 条）
反应条件
hydrogenchloride in 1,4-dioxane
1) 60-70 deg C, 6 h, 2) 60-90 deg C, 8 h;
参考文献
Mormann, Werner; Hoffmann, Silke; Hoffmann, Walter
Chemische Berichte, 1987 , vol. 120, p. 285 - 290
反应条件
hydrogenchloride in 1,4-dioxane
参考文献
Iwakura,Y. et al.
Journal of Organic Chemistry, 1966 , vol. 31, p. 142 - 146
反应条件
1: methyl 3-aminopropanoate hydrochloride With carbon dioxide; 1,1,1,3,3,3-hexamethyl-disilazane
5 h; Heating;
2: phosgene in toluene
T=25°C; Further stages.;
参考文献
Lebedev; Lebedeva; Sheludyakov; Ovcharuk; Kovaleva; Ustinova
Russian Journal of General Chemistry, 2006 , vol. 76, # 7 p. 1069 - 1080
反应条件
1: ethyl 3-aminopropanoate hydrochloride With carbon dioxide; 1,1,1,3,3,3-hexamethyl-disilazane
5 h; Heating;
2: phosgene in toluene
T=25°C; Further stages.;
参考文献
Lebedev; Lebedeva; Sheludyakov; Ovcharuk; Kovaleva; Ustinova
Russian Journal of General Chemistry, 2006 , vol. 76, # 7 p. 1069 - 1080
反应条件
thionyl chloride in tetrachloromethane
参考文献
Kricheldorf,H.R.
Chemische Berichte, 1971 , vol. 104, p. 87 - 91
参考文献
Kurita,K. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 2070 - 2071
参考文献
Mormann, W.; Hissmann, E.
Tetrahedron Letters, 1987 , vol. 28, # 27 p. 3087 - 3090
参考文献
Mormann, W.; Hissmann, E.
Tetrahedron Letters, 1987 , vol. 28, # 27 p. 3087 - 3090
