2,2-二氯环丙烷-1-甲腈合成路线 (共 10 条)
反应条件
sodium hydroxide; tetrabutylammomium bromide in water; benzene T=25 - 30°C; Title compound not separated from byproducts.;
参考文献
Jonczyk, Andrzej; Kocmierowski, Tomasz; Zdrojewski, Tadeusz
New Journal of Chemistry, 2003 , vol. 27, # 2 p. 295 - 299
反应条件
in methanol T=15 - 20°C; 0.333333 h;
参考文献
Kulinkovich, O. G.; Tishchenko, I. G.; Romashin, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 213 - 216
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 242 - 246
反应条件
sodium iodide in ethylene glycol dimethyl ether
参考文献
Seyferth,D. et al.
Journal of the American Chemical Society, 1965 , vol. 87, # 3 p. 681 - 682
反应条件
phosphorus pentachloride
heating under water-jet pump vacuum;
参考文献
Kulinkovich, O. G.; Tishchenko, I. G.; Romashin, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 213 - 216
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 242 - 246
反应条件
1: (phenyl)(trichloromethyl)mercury in benzene
Reflux;
2: acrylonitrile
参考文献
Moss, Robert A.; Zhang, Min; Krogh-Jespersen, Karsten
Organic Letters, 2009 , vol. 11, # 9 p. 1947 - 1950
反应条件
in pentane
T=24.1°C; Kinetics;
参考文献
Moss, Robert A.; Zhang, Min; Krogh-Jespersen, Karsten
Organic Letters, 2009 , vol. 11, # 9 p. 1947 - 1950
反应条件
sodium hydroxide; tetrabutylammomium bromide in water; benzene
T=25 - 30°C; Title compound not separated from byproducts.;
参考文献
Jonczyk, Andrzej; Kocmierowski, Tomasz; Zdrojewski, Tadeusz
New Journal of Chemistry, 2003 , vol. 27, # 2 p. 295 - 299
反应条件
in ethanol
T=15 - 20°C; 0.333333 h;
参考文献
Kulinkovich, O. G.; Tishchenko, I. G.; Romashin, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 213 - 216
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 242 - 246
反应条件
sodium hydroxide; tetrabutylammomium bromide in water; benzene
2 h;
参考文献
Jonczyk, Andrzej; Kocmierowski, Tomasz; Zdrojewski, Tadeusz
New Journal of Chemistry, 2003 , vol. 27, # 2 p. 295 - 299
反应条件
in methanol
T=15 - 20°C; 0.5 h;
参考文献
Kulinkovich, O. G.; Tishchenko, I. G.; Romashin, Yu. N.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 213 - 216
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 242 - 246