环氧乙烷-2-基甲基丙酸酯合成路线 (共 4 条)
反应条件
15-crown-5 in acetonitrile
13 h; Ambient temperature;
参考文献
Nair, Ranjeet V.; Patil, Prashant N.; Salunkhe, Manikrao M.
Synthetic Communications, 1999 , vol. 29, # 15 p. 2559 - 2566
反应条件
methanol; magnesium
3 h; Ambient temperature;
参考文献
Hudlicky, T.; Sinai-Zingde, G.; Natchus, M. G.
Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5287 - 5290
反应条件
triethylamine in toluene
T=0°C; 0.833333 h;
参考文献
Davies, Alwyn G.; Hawari, Jalal A.-A.; Muggleton, Brenda; Tse, Man-Wing
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 1132 - 1137
反应条件
potassium carbonate; 1.) Sn-P
1.) benzene, reflux, 20 h; 2.) acetone, reflux, 6 h; Yield given. Multistep reaction;
参考文献
Otera, Junzo; Matsuzaki, Shinjiro
Synthesis, 1986 , # 12 p. 1019 - 1020