反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '1736662', constants.ctx, '0')">acetic acid methyl ester</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '8136861', constants.ctx, '0')">lithium hexamethyldisilazane</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=-78°C; 0.5 h; Inert atmosphere; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1209232', constants.ctx, '0')">trimethylsilyl chloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br />T=-78°C; 1.83333 h; Inert atmosphere; <br /> <br />
参考文献
Kholod, Inga; Vallat, Olivier; Buciumas, Ana-Maria; Neier, Reinhard Arkivoc, 2014 , vol. 2014, # 3 p. 256 - 273
