2,4,6-三(三氟甲基)-1,3,5-三嗪合成路线 （共 20 条）
反应条件
SbF3; antimony trichloride; chlorine
参考文献
Norton
Journal of the American Chemical Society, 1950 , vol. 72, p. 3527
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McBee et al.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 389
反应条件
in dichloromethane T=60°C; P=7500600 Torr; 65 h; other solvent;
参考文献
Koppes, William M.; Adolph, Horst G.
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 406 - 412
反应条件
hydrogenchloride T=10 - 100°C; unter Druck;
参考文献
Reilly; Brown
Journal of Organic Chemistry, 1957 , vol. 22, p. 698
反应条件
SbF5 Ambient temperature;
参考文献
Buerger, H.; Koeplin, R.; Pawelke, G.; Krueger, C.
Journal of Fluorine Chemistry, 1983 , vol. 22, p. 175 - 184
反应条件
in dichloromethane T=60°C; P=7500600 Torr; 23 h;
参考文献
Koppes, William M.; Adolph, Horst G.
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 406 - 412
反应条件
1.) Et2O, -20 deg C to 25 deg C, 2.) 97 deg C, 162 torr, 2 h; 110 deg C, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Norris, William P.; Merwin, Lawrence H.; Ostrom, Gregory S.; Gilardi, Richard D.
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9070 - 9075
参考文献
Norton
Journal of the American Chemical Society, 1950 , vol. 72, p. 3527
Full Text View citing articles Show Details
McBee et al.
Industrial and Engineering Chemistry, 1937 , vol. 39, p. 391
反应条件
hydrogen iodide T=200°C; 24 h; Product distributionMechanism;
参考文献
Eltoum, Ahmed O. A.; O'Reilly, Neil J.; Tipping, Anthony E.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 101 - 110
参考文献
Bissell; Spenger
Journal of Organic Chemistry, 1959 , vol. 24, p. 1147
反应条件
multistep: 1.) Et2O, -20 deg C to 25 deg C, 2.) C6D6, 117 deg C, 30 min; Rate constantProduct distribution;
参考文献
Norris, William P.; Merwin, Lawrence H.; Ostrom, Gregory S.; Gilardi, Richard D.
Journal of Organic Chemistry, 1997 , vol. 62, # 26 p. 9070 - 9075
