2-(4-氯苄基)乙酰乙酸乙酯合成路线 (共 6 条)
反应条件
potassium hydroxide; tetrabutyl-ammonium chloride; potassium carbonate 0.0666667 h; Irradiation;
参考文献
Runhua, Deng; Yuliang, Wang; Yaozhong, Jiang
Synthetic Communications, 1994 , vol. 24, # 1 p. 111 - 116
反应条件
1: ethyl acetoacetate With potassium tert-butylate in tetrahydrofuran; tert-butyl alcohol T=20°C; 0.5 h; 2: 4-chloro-benzyl chloride in tetrahydrofuran; tert-butyl alcohol T=70°C;
参考文献
WO2007/144625 A1, ;
Page/Page column 40 ;
反应条件
K5[CoW12O40]*3H2O in neat (no solvent) T=80°C; 0.333333 h;
参考文献
Rafiee, Ezzat; Kahrizi, Masoud; Joshaghani, Mohammad
Chinese Chemical Letters, 2012 , vol. 23, # 12 p. 1363 - 1366
反应条件
12-tungestocobaltic acid supported on nano silica T=80°C; 0.0833333 h; neat (no solvent);
参考文献
Rafiee, Ezzat; Khodayari, Maryam; Kahrizi, Masoud; Tayebee, Reza
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 358, p. 121 - 128
参考文献
Journal of the American Chemical Society, , vol. 73, p. 3758,3760
反应条件
(i) K, EtOH, (ii) /BRN= 471558/, HMPA; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 34, p. 1969 - 1973