4-氟-N-苯基苯甲酰胺合成路线 （共 23 条）
反应条件
oxygen; lithium hydroxide hydrate in water
T=50°C; 12 h;
参考文献
Wang, Ye; Zhu, Dapeng; Tang, Lin; Wang, Sujing; Wang, Zhiyong
Angewandte Chemie - International Edition, 2011 , vol. 50, # 38 p. 8917 - 8921
反应条件
copper(l) iodide; acetaldehyde oxime; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=120°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Dong-Xue; Xiang, Shi-Kai; Hu, Hao; Tan, Wen; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Tetrahedron, 2013 , vol. 69, # 47 p. 10022 - 10029
反应条件
in N,N-dimethyl-formamide
1.) 48 h; 2.) 0 deg C, 15 min;
参考文献
Vigorita; Saporito; Previtera; et al.
Farmaco, Edizione Scientifica, 1986 , vol. 41, # 2 p. 168 - 174
反应条件
1: aniline With C12H30NaO6(1+)*C56H84O4Sm(1-) in tetrahydrofuran
0.5 h; Inert atmosphere;
2: 4-fluorobenzaldehyde in tetrahydrofuran
T=25°C; 3 h; Inert atmosphere;
参考文献
Li, Junmei; Xu, Fan; Zhang, Yong; Shen, Qi
Journal of Organic Chemistry, 2009 , vol. 74, # 6 p. 2575 - 2577
反应条件
palladium 10 on activated carbon; 1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=130°C; P=6723.1 Torr; 0.333333 h; Microwave irradiation;
参考文献
Salvadori, Jessica; Balducci, Evita; Zaza, Silvia; Petricci, Elena; Taddei, Maurizio
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 1841 - 1847
反应条件
di-tert-butyl peroxide; potassium hydroxide in chlorobenzene
T=140°C; 24 h;
参考文献
Xiao, Fuhong; Liu, Yong; Tang, Chenglin; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 4 p. 984 - 987
反应条件
1,10-phenanthroline; oxygen; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in dimethyl sulfoxide
T=140°C; 72 h; Schlenk technique;
参考文献
Xu, Mei; Zhang, Xiao-Hong; Shao, Yin-Lin; Han, Jiang-Sheng; Zhong, Ping
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2665 - 2670,6
Title/Abstract Full Text Show Details
Xu, Mei; Zhang, Xiao-Hong; Shao, Yin-Lin; Han, Jiang-Sheng; Zhong, Ping
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2665 - 2670
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=60°C; 0.05 h; Microwave irradiation;
参考文献
Kumar, Katari Naresh; Sreeramamurthy, Kintali; Palle, Sadananda; Mukkanti, Khagga; Das, Parthasarathi
Tetrahedron Letters, 2010 , vol. 51, # 6 p. 899 - 902
反应条件
potassium carbonate; aniline in water
参考文献
Mills; Randell L.
Patent: US5428163 A1, 1995 ;
反应条件
2-(di-tert-butylphosphino)-2'-isopropoxy-1,1'-binaphthyl; caesium carbonate; bis(dibenzylideneacetone)-palladium(0) in tert-butyl alcohol
T=100°C; 20 h; Inert atmosphere;
参考文献
Ma, Fangfang; Xie, Xiaomin; Zhang, Lei; Peng, Zhiyong; Ding, Lina; Fu, Lei; Zhang, Zhaoguo
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5279 - 5285
