4-[3-(4,4,5,5-四甲基-1,3,2-二氧硼烷-2-基)苄基]吗啉合成路线 （共 8 条）
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
PS-NMM in tetrahydrofuran T=150°C; 0.25 h; Microwave irradiationin air;
参考文献
Spencer, John; Baltus, Christine B.; Patel, Hiren; Press, Neil J.; Callear, Samantha K.; Male, Louise; Coles, Simon J.
ACS Combinatorial Science, 2011 , vol. 13, # 1 p. 24 - 31
反应条件
potassium acetate in water; dimethyl sulfoxide; ethyl acetate; toluene
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate in dimethyl sulfoxide
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 20 p. 2989 - 2992
反应条件
potassium acetate in dichloromethane; dimethyl sulfoxide
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: NaCNBH3; AcOH / ethanol 2: PdCl2dppf*CH2Cl2; KOAc / dimethylsulfoxide View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 12, # 20 p. 2989 - 2992
