2-(3-(苄氧基)-4-甲氧基苯基)乙胺合成路线 （共 14 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 24 h;
参考文献
Ploypradith, Poonsakdi; Petchmanee, Thaninee; Sahakitpichan, Poolsak; Litvinas, Nichole D.; Ruchirawat, Somsak
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9440 - 9448
反应条件
nickel; hydrazine hydrate in methanol; water T=0 - 40°C; 1 h;
参考文献
Leese, Mathew P.; Jourdan, Fabrice L.; Major, Meriel R.; Dohle, Wolfgang; Hamel, Ernest; Ferrandis, Eric; Fiore, Ann; Kasprzyk, Philip G.; Potter, Barry V. L.
ChemMedChem, 2014 , vol. 9, # 1 p. 85 - 108
反应条件
1: K2CO3 / acetone / 6 h / Heating 2: 80 percent / AcOH; ethylenediamine / 20 °C 3: 93 percent / LAH / tetrahydrofuran / 24 h / 20 °C View Scheme
参考文献
Cabedo, Nuria; Protais, Philippe; Cassels, Bruce K.; Cortes, Diego
Journal of Natural Products, 1998 , vol. 61, # 6 p. 709 - 712
反应条件
1: 80 percent / AcOH; ethylenediamine / 20 °C 2: 93 percent / LAH / tetrahydrofuran / 24 h / 20 °C View Scheme
参考文献
Bermejo, Almudena; Andreu, Inmaculada; Suvire, Fernando; Leonce, Stephane; Caignard, Daniel H.; Renard, Pierre; Pierre, Alain; Enriz, Ricardo D.; Cortes, Diego; Cabedo, Nuria
Journal of Medicinal Chemistry, 2002 , vol. 45, # 23 p. 5058 - 5068
反应条件
1: 94 percent / K2CO3 / ethanol / 5 h / Heating 2: 88 percent / NH4OAc; AcOH / 4 h / Heating 3: 63 percent / LiAlH4 / diethyl ether; tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Andreu, Inmaculada; Cabedo, Nuria; Atassi, Ghanem; Pierre, Alain; Caignard, Daniel H; Renard, Pierre; Cortes, Diego; Bermejo, Almudena
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 757 - 759
反应条件
1: K2CO3 / acetone / 6 h / Heating 2: 80 percent / AcOH; ethylenediamine / 20 °C 3: 93 percent / LAH / tetrahydrofuran / 24 h / 20 °C View Scheme
参考文献
Crestey, Francois; Jensen, Anders A.; Borch, Morten; Andreasen, Jesper Tobias; Andersen, Jacob; Balle, Thomas; Kristensen, Jesper Langgaard
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9673 - 9682
反应条件
1: 100 percent / NH4OAc / Heating 2: 78 percent / LiAlH4 / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Pinet; Chavant; Averbuch-Pouchot; Vallee
Journal of Chemical Research - Part S, 2001 , # 2 p. 65 - 67
参考文献
Spaeth; Orechoff; Kuffner
Chemische Berichte, 1934 , vol. 67, p. 1214,1216
反应条件
1: 5percent aq. NaOH / CH2Cl2 / 2 h / 20 °C 2: conc. HCl / ethanol / 4 h / Heating View Scheme
参考文献
Bermejo, Almudena; Andreu, Inmaculada; Suvire, Fernando; Leonce, Stephane; Caignard, Daniel H.; Renard, Pierre; Pierre, Alain; Enriz, Ricardo D.; Cortes, Diego; Cabedo, Nuria
Journal of Medicinal Chemistry, 2002 , vol. 45, # 23 p. 5058 - 5068
反应条件
1: 89 percent / ethanol / 7 h / Heating 2: 1) PCl5, 2) NaBH4 / 1) CHCl3, room temperature, 1 h, 2) CH3OH 3: 76 percent / conc. HCl / ethanol / 2 h / Heating View Scheme
参考文献
Mali, R. S.; Yeola, Suresh N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 79 - 80
