2-甲基-1,2-二氢二氮杂萘合成路线 （共 5 条）
反应条件
sodium hydroxide; potassium carbonate in water T=120°C; P=2068.59 - 4137.18 Torr; 0.333333 h; microwave irradiation;
参考文献
Ju, Yuhong; Varma, Rajender S.
Tetrahedron Letters, 2005 , vol. 46, # 36 p. 6011 - 6014
反应条件
sodium tetrahydroborate in water
参考文献
Ruxer; Mauger; Benard; Lachoux
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 2 p. 643 - 654
反应条件
1: 98 percent / methanol / 3 h / Heating 2: sodium borohydride / H2O / 3 h View Scheme
参考文献
Nguyen, Minh Tho; Clarke, Leo F.; Hegarty, Anthony F.
Journal of Organic Chemistry, 1990 , vol. 55, # 25 p. 6177 - 6183
反应条件
in water; acetonitrile T=25°C; pH 7.0; other phthalazinium cations; Rate constantMechanism;
参考文献
Bunting, John W.; Chew, Vivian S. F.; Chu, Gary
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2303 - 2307
反应条件
1: 61 percent / methanol / 3 h / Heating
2: pyrrolidine / methanol / 25 °C / or triethylamine, N-methylpiperidine, morpholine, N-ethylmorpholine, N-methylmorpholine
View Scheme
参考文献
Nguyen, Minh Tho; Clarke, Leo F.; Hegarty, Anthony F.
Journal of Organic Chemistry, 1990 , vol. 55, # 25 p. 6177 - 6183
