4-(4-甲基苯基)苯甲醛合成路线 （共 31 条）
反应条件
1.1: 75 percent / NiCl2; 2,2'-bipyridine; PPh3 / Zn / dimethylformamide / 5 h / 90 °C 2.1: NBS / benzene / 12 h / Heating 3.1: hexamethylenetetramine / CHCl3 / 12 h / Heating 3.2: 25 percent / aq. AcOH / 2 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 48 p. 14410 - 14415
反应条件
1H-imidazole; [bis(acetoxy)iodo]benzene; Cu(AAOPD) in acetonitrile T=20°C; 4.41667 h;
参考文献
Soleymani, Reza; Taheri, Milad; HOSEYNALIBEYGl, Marziye; Daryani, Mehdi
Oriental Journal of Chemistry, 2012 , vol. 28, # 2 p. 857 - 866,10
反应条件
1: With 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in chloroform 12 h; Heating; 2: With acetic acid 2 h; Heating; Further stages.;
参考文献
An, Byeong-Kwan; Kwon, Soon-Ki; Jung, Sang-Don; Park, Soo Young
Journal of the American Chemical Society, 2002 , vol. 124, # 48 p. 14410 - 14415
反应条件
NiCl2(PCy3)2 in benzene T=25°C; 1 h;
参考文献
Hirner, Joshua J.; Blum, Suzanne A.
Organometallics, 2011 , vol. 30, # 6 p. 1299 - 1302
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 0.25 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 17 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
potassium phosphate; palladium diacetate; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=65°C; Suzuki-Miyaura cross-coupling; 6 h; Reactivity;
参考文献
US2009/30238 A1, ;
Page/Page column 12-13 ;
反应条件
potassium phosphate; palladium diacetate; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=65°C; Suzuki-Miyaura cross-coupling; 6 h; Reactivity;
参考文献
US2009/30238 A1, ;
Page/Page column 12-13 ;
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy in tetrahydrofuran T=63°C; 1 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI in tetrahydrofuran; benzene T=63°C; 3 h;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
