N-乙酰-L-苯丙氨酸甲酯合成路线 (共 84 条)
反应条件
1: methyl (S)-2-acetamido-3-phenylpropanoate With triphenyl phosphite; chlorine; triethylamine in tetrahydrofuran T=-30°C; 2: 2-methyl-propan-1-ol in tetrahydrofuran T=-30 - 20°C; 3: With water
参考文献
Spaggiari, Alberto; Blaszczak, Larry C.; Prati, Fabio
Organic Letters, 2004 , vol. 6, # 22 p. 3885 - 3888
反应条件
in methanol T=0°C; 12 h;
参考文献
Hlavacek, Jan; Fric, Ivo; Budesinsky, Milos; Blaha, Karel
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 11A p. 2473 - 2494
反应条件
modified subtilisin Carlsberg Type VIII in carbon dioxide; water T=47°C; P=85329.4 Torr;
参考文献
Smallridge, Andrew J.; Trewhella, Maurie A.; Wang
Australian Journal of Chemistry, 2002 , vol. 55, # 4 p. 259 - 262
反应条件
sodium carbonate in methanol; water 4 h;
参考文献
Kaestle; Anwer; Audhya; Goldstein
Tetrahedron Letters, 1991 , vol. 32, # 3 p. 327 - 330