3-(1-萘基氧基)-1,2-丙二醇合成路线 (共 22 条)
反应条件
perchloric acid in water T=80°C;
参考文献
Dishong, Dennis M.; Diamond, Craig J.; Cinoman, Michael I.; Gokel, Geoge W.
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 586 - 593
反应条件
AD-mix-β in water; tert-butyl alcohol T=0°C;
参考文献
Wang; Zhang; Sharpless
Tetrahedron Letters, 1993 , vol. 34, # 14 p. 2267 - 2270
反应条件
sodium hydroxide in ethanol 2 h; Heating;
参考文献
Egri, Gabriella; Kolbert, Attila; Balint, Jozsef; Fogassy, Elemer; Novak, Lajos; Poppe, Laszlo
Tetrahedron Asymmetry, 1998 , vol. 9, # 2 p. 271 - 283
反应条件
hydrogenchloride in methanol; water; N,N-dimethyl-formamide
参考文献
Wake Forest University
Patent: US5614548 A1, 1997 ;
反应条件
5 palladium on charcoal in neat (no solvent) T=150°C; 60 h; Inert atmosphereSealed tubeGreen chemistry; regioselective reaction;
参考文献
Sutter, Marc; Lafon, Romain; Raoul, Yann; Metay, Estelle; Lemaire, Marc
European Journal of Organic Chemistry, 2013 , # 26 p. 5902 - 5916
反应条件
1: 2.) 50percent aq. NaOH / 1.) 80 deg C, 2.) 4 h 2: 46 percent / 72percent HClO4 / H2O / 80 °C View Scheme
参考文献
Wang; Chen; Liu; Wong
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1917 - 1920
反应条件
hydrogen; palladium on activated charcoal
参考文献
Carlsen, Per H.; Aase, Kristin J.
Acta Chemica Scandinavica, 1993 , vol. 47, # 6 p. 617 - 619
反应条件
triethylamine in ethanol Heating;
参考文献
Bredikhina; Savel'ev; Bredikhin
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 2 p. 213 - 219
反应条件
Bacillus megaterium ECU1001 epoxide hydrolase in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 2 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Zhao, Jing; Chu, Yan-Yan; Li, Ai-Tao; Ju, Xin; Kong, Xu-Dong; Pan, Jiang; Tang, Yun; Xu, Jian-He
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1510 - 1518
反应条件
sodium acetate T=200 - 210°C;
参考文献
Truscello, Ada M.; Gambarotti, Cristian; Lauria, Mirvana; Auricchio, Sergio; Leonardi, Gabriella; Shisodia, Suresh U.; Citterio, Attilio
Green Chemistry, 2013 , vol. 15, # 3 p. 625 - 628