(3-溴丙基)三苯基溴化磷合成路线 （共 51 条）
反应条件
(i) NaH, (ii) /BRN= 385772/; Multistep reaction;
参考文献
Wang, Bin; Shen, Yu-Mei; Shi, Yian
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9519 - 9521
反应条件
(i) NaH, (ii) /BRN= 471382/; Multistep reaction;
参考文献
Wang, Bin; Shen, Yu-Mei; Shi, Yian
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9519 - 9521
反应条件
1: 94 percent / dimethylformamide / 4 h / Heating
2: 92 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
3: 1.) trichlorosilane, triethylamine 2.) 50percent aqueous sodium hydroxide / 1.) toluene, 5 min then reflux, 2 h 2.) toluene, ice cooling, 1 h
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
反应条件
1: 94 percent / dimethylformamide / 4 h / Heating
2: 92 percent / 20percent aqueous sodium hydroxide / 1 h / Heating
3: sulphur / toluene / 2 h
View Scheme
参考文献
Benn, Roger F.; Briggs, Josie C.; McAuliffe, Charles A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 293 - 296
参考文献
Fournet, Guy; Balme, Genevieve; Gore, Jacques
Tetrahedron, 1988 , vol. 44, # 18 p. 5809 - 5820
反应条件
(i) KOtBu, DMSO, (ii) /BRN= 605330/; Multistep reaction;
参考文献
Eckes,L.; Hanack,M.
Chemische Berichte, 1978 , vol. 111, p. 1253 - 1263
反应条件
(i) NaH, DMF, (ii) /BRN= 635749/; Multistep reaction;
参考文献
Rousseau,G. et al.
Tetrahedron, 1976 , vol. 32, p. 2533 - 2537
反应条件
potassium tert-butylate in tetrahydrofuran
参考文献
Wang, Bin; Shen, Yu-Mei; Shi, Yian
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9519 - 9521
反应条件
(i) NaH, (ii) /BRN= 605842/; Multistep reaction;
参考文献
Wang, Bin; Shen, Yu-Mei; Shi, Yian
Journal of Organic Chemistry, 2006 , vol. 71, # 25 p. 9519 - 9521
参考文献
Dunkelblum,E.
Tetrahedron, 1974 , vol. 30, p. 3991 - 3996
