(3-溴丙基)三苯基溴化磷合成路线 （共 51 条）
反应条件
in xylene T=130°C; 16 h;
参考文献
Siriwardana, Amal I.; Nakamura, Itaru; Yamamoto, Yoshinori
Tetrahedron Letters, 2003 , vol. 44, # 24 p. 4547 - 4550
反应条件
hydrogen bromide 5 h; Heating;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 23 p. 4345 - 4351
反应条件
sodium hydride in tetrahydrofuran T=60°C;
参考文献
Chen, Gen-Qiang; Tang, Xiang-Ying; Shi, Min
European Journal of Organic Chemistry, 2014 , vol. 2014, # 1 p. 194 - 197
反应条件
1: (3-bromopropyl)triphenylphosphinium bromide With potassium tert-butylate in tetrahydrofuran 1.16667 h; Reflux; 2: 4-chlorobenzaldehyde in tetrahydrofuran 4 h; Reflux;
参考文献
SYNGENTA PARTICIPATIONS AG; O'SULLIVAN, Anthony, Cornelius; LOISELEUR, Olivier; STAIGER, Roman; LUKSCH, Torsten; PITTERNA, Thomas
Patent: WO2013/143811 A1, 2013 ;
Location in patent: Page/Page column 79 ;
反应条件
in ethanol; water T=20 - 100°C; Sealed tube;
参考文献
NEKTAR THERAPEUTICS; RIGGS-SAUTHIER, Jennifer; DENG, Bo-Liang; GURSAHANI, Hema
Patent: WO2012/79017 A1, 2012 ;
Location in patent: Page/Page column 68 ;
WO 2012/079017 A1
参考文献
Balema, Viktor P.; Wiench, Jerzy W.; Pruski, Marek; Pecharsky, Vitalij K.
Chemical Communications, 2002 , # 7 p. 724 - 725
反应条件
in water; acetone 15 h; Heating;
参考文献
Hercouet, A.; Corre, M. Le
Tetrahedron, 1981 , vol. 37, # 16 p. 2855 - 2860
反应条件
sodium hydroxide in water 2 h, reflux; 12 h, room temp.;
参考文献
Maercker, Adalbert; Daub, Volker E. E.
Tetrahedron, 1994 , vol. 50, # 8 p. 2439 - 2458
反应条件
sodium hydride 1.) glyme, ethanol, 6 h, 70 deg C, 2.) 12 h, 80 deg C; Yield given. Multistep reaction;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
(i) NaH, DMF, (ii) /BRN= 385735/; Multistep reaction;
参考文献
Rousseau,G. et al.
Tetrahedron, 1976 , vol. 32, p. 2533 - 2537
