2,4-二甲基-6-苯基-1,3,5-三嗪合成路线 (共 6 条)
反应条件
caesium carbonate in dimethyl sulfoxide T=90°C; 12 h; Inert atmosphere;
参考文献
Biswas, Subhasish; Batra, Sanjay
European Journal of Organic Chemistry, 2012 , # 18 p. 3492 - 3499
反应条件
potassium tert-butylate in tetrahydrofuran T=67°C; 16 h;
参考文献
Chen; Dagnino R.; McCarthy
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8428 - 8430
反应条件
1: 1 h / 80 °C 2: 40 percent / t-BuOK / tetrahydrofuran / 16 h / 67 °C View Scheme
参考文献
Chen; Dagnino R.; McCarthy
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8428 - 8430
反应条件
1: N-chlorosuccinimide / CH2Cl2 / 0.25 h 2: NaOMe / methanol / 1 h / Heating View Scheme
参考文献
Malecot, Yves-Michel; Ripoll, Jean-Louis; Thuillier, Andre
Journal of Chemical Research, Miniprint, 1983 , # 4 p. 959 - 993
反应条件
in acetonitrile 2.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Pavlik, James W.; Changtong, Chuchawin; Vikki
Journal of Organic Chemistry, 2003 , vol. 68, # 12 p. 4855 - 4861
反应条件
methanol; copper diacetate; zinc
参考文献
Grundmann et al.
Chemische Berichte, 1953 , vol. 86, p. 181,184