1,3-二溴-2-甲基丙-1-烯合成路线 (共 14 条)
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane 1 h; Heating;
参考文献
Fischetti, William; Mak, K. Tim; Stakem, F. Gregory; Kim, Jin-Il; Rheingold, Arnold L.; Heck, Richard F.
Journal of Organic Chemistry, 1983 , vol. 48, # 7 p. 948 - 955
反应条件
phosphorus tribromide in diethyl ether T=0 - 25°C; 4.5 h;
参考文献
Reyes, Samuel; Huigens Iii, Robert W.; Su, Zhaoming; Simon, Michel L.; Melander, Christian
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 8 p. 3041 - 3049
反应条件
potassium hydroxide T=145 - 150°C; P=100 Torr;
参考文献
Mereshkowski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1914 , vol. 46, p. 118
Chem. Zentralbl., 1914 , vol. 85, # I p. 2160
反应条件
bromine in tetrachloromethane T=-15°C;
参考文献
Nesmeyanova, O. A.; Kudryatseva, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 11 p. 2324
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 11 p. 2629 - 2630
反应条件
potassium hydroxide T=145 - 150°C; P=100 Torr;
参考文献
Kirrmann
Bulletin de la Societe Chimique de France, 1930 , vol. <4>47, p. 844
反应条件
sodium acetate 10 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kartashov, V. R.; Skorobogatova, E. V.; Afanas'ev, P. S.; Chertkov, V. A.; Sergeev, N. M.; et al.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 9.1 p. 1639 - 1648
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 9 p. 1861 - 1872
反应条件
in methanol 3 h; Heating;
参考文献
Walsh,R.A.; Bottini,A.T.
Journal of Organic Chemistry, 1970 , vol. 35, p. 1086 - 1092
反应条件
sodium 3 h; Heating;
参考文献
Walsh,R.A.; Bottini,A.T.
Journal of Organic Chemistry, 1970 , vol. 35, p. 1086 - 1092
参考文献
Walsh,R.A.; Bottini,A.T.
Journal of Organic Chemistry, 1970 , vol. 35, p. 1086 - 1092
反应条件
(i), (ii) /BRN= 3556712/, THF; Multistep reaction;
参考文献
Walsh,R.A.; Bottini,A.T.
Journal of Organic Chemistry, 1970 , vol. 35, p. 1086 - 1092