1-溴-2,2-二氟乙烷合成路线 （共 32 条）
反应条件
sodium hydrogencarbonate
参考文献
Dickey et al.
Industrial and Engineering Chemistry, 1954 , vol. 46, p. 2213,2217
反应条件
sodium iodide in N,N-dimethyl-formamide T=130°C; 18 h;
参考文献
SOLVAY (Societe Anonyme)
Patent: WO2009/40367 A1, 2009 ;
Location in patent: Page/Page column 10 ;
反应条件
1: potassium acetate With sulfolane in water T=100°C; Inert atmosphere; 2: 2-bromo-1,1-difluoroethane T=20 - 135°C;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY; PETROV, Viacheslav, A.; DUBOIS, Charles, J.
Patent: WO2013/180782 A1, 2013 ;
Location in patent: Page/Page column 23; 24; 25 ;
反应条件
in N,N-dimethyl-formamide T=130°C; 40 h; Product distribution / selectivity;
参考文献
SOLVAY (Societe Anonyme)
Patent: WO2009/40367 A1, 2009 ;
Location in patent: Page/Page column 10-12 ;
反应条件
potassium hydroxide in methanol
1 h; Heating;
参考文献
Trachsel, Daniel
Helvetica Chimica Acta, 2003 , vol. 86, # 7 p. 2610 - 2619
反应条件
ethanol; zinc
T=50°C;
参考文献
Swarts
Chem. Zentralbl., 1901 , vol. 72, # II p. 804
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Swarts
Chem. Zentralbl., 1909 , vol. 80, # II p. 1414
参考文献
Swarts
Chem. Zentralbl., 1901 , vol. 72, # II p. 804
参考文献
Swarts
Chem. Zentralbl., 1904 , vol. 75, # II p. 1377
参考文献
Swarts
Chem. Zentralbl., 1901 , vol. 72, # II p. 804
反应条件
ethanol; ammonia
T=125 - 145°C;
参考文献
Swarts
Chem. Zentralbl., 1904 , vol. 75, # II p. 944
