N-(2-氰基乙基)-邻苯二甲酰亚胺合成路线 (共 15 条)
反应条件
in dimethyl sulfoxide T=65°C; 6 h;
参考文献
Martinkus; Tann; Gould
Tetrahedron, 1983 , vol. 39, # 21 p. 3493 - 3505
反应条件
bromine trifluoride in monofluoro-trichloromethane T=0°C; 0.0333333 h;
参考文献
Sasson, Revital; Rozen, Shlomo
Organic Letters, 2005 , vol. 7, # 11 p. 2177 - 2179
反应条件
triethylamine; tetra-(n-butyl)ammonium iodide in N,N-dimethyl-formamide 5 h; Heating;
参考文献
Soltani Rad, Mohammad Navid; Khalafi-Nezhad, Ali; Behrouz, Somayeh; Faghihi, Mohammad Ali
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6779 - 6784
反应条件
potassium phtalimide Michael addition; 3 h; Inert atmosphereReflux;
参考文献
Dawadi, Prativa B. S.; Lugtenburg, Johan
European Journal of Organic Chemistry, 2008 , # 13 p. 2288 - 2292
参考文献
Buc
Journal of the American Chemical Society, 1947 , vol. 69, p. 254
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Chodroff; Kapp; Beckmann
Journal of the American Chemical Society, 1947 , vol. 69, p. 256
反应条件
trifluoroacetic acid; trifluoroacetic anhydride; sodium nitrite T=20°C; nitrosative cleavage;
参考文献
Smushkevich, Y. I.; Smushkevich, V. Y.; Usorov, M. I.
Journal of Chemical Research, Miniprint, 1999 , # 7 p. 1727 - 1736
反应条件
1: 2-methyl-pentanone-(4) 2: 200 °C View Scheme
参考文献
Chodroff; Kapp; Beckmann
Journal of the American Chemical Society, 1947 , vol. 69, p. 256
参考文献
Chodroff; Kapp; Beckmann
Journal of the American Chemical Society, 1947 , vol. 69, p. 256
反应条件
acetic acid; methylhydrazine 0.0833333 h; Heating;
参考文献
Liebscher, Juergen; Pragst, Fritz; Anders, Sabine; Bechstein, Ute; Bohrisch, Joerg; et al.
Journal fuer Praktische Chemie (Leipzig), 1988 , vol. 330, # 5 p. 847 - 850
反应条件
(i) aq. HCl, (ii) /BRN= 1098229/, SOCl2; Multistep reaction;
参考文献
Becker,H.G.O.
Journal fuer Praktische Chemie (Leipzig), 1961 , vol. 12, p. 294 - 305