2-(2-硝基苯基)苯胺合成路线 (共 18 条)
反应条件
formic acid; triethylamine; palladium on activated charcoal T=100°C; 1 h;
参考文献
Terpko, Marc O.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4992 - 4993
反应条件
potassium dihydrogenphosphate; tetrabutylammomium bromide; palladium diacetate in water; N,N-dimethyl-formamide T=100°C; Suzuki cross-coupling;
参考文献
Gonzalez, Raquel Rodriguez; Liguori, Lucia; Carrillo, Alberto Martinez; Bjorsvik, Hans-Rene
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9591 - 9594
反应条件
potassium dihydrogenphosphate; tetrabutylammomium bromide; palladium diacetate in water; N,N-dimethyl-formamide T=100°C; Suzuki cross-coupling; 48 h;
参考文献
Gonzalez, Raquel Rodriguez; Liguori, Lucia; Carrillo, Alberto Martinez; Bjorsvik, Hans-Rene
Journal of Organic Chemistry, 2005 , vol. 70, # 23 p. 9591 - 9594
反应条件
1: copper / 60 °C / |Schlenk technique; |Inert atmosphere 2: NaSx / ethanol / 6 h / |Schlenk technique; |Inert atmosphere; |Reflux View Scheme
参考文献
Yi, Wei; Ma, Haiyan
Dalton Transactions, 2014 , vol. 43, # 13 p. 5200 - 5210
反应条件
1: hydrogenchloride; potassium iodide; sodium nitrite / -5 - 0 °C / |Schlenk technique; |Inert atmosphere 2: copper / 60 °C / |Schlenk technique; |Inert atmosphere 3: NaSx / ethanol / 6 h / |Schlenk technique; |Inert atmosphere; |Reflux View Scheme
参考文献
Yi, Wei; Ma, Haiyan
Dalton Transactions, 2014 , vol. 43, # 13 p. 5200 - 5210
反应条件
potassium hypobromide
参考文献
Angelini
Annali di Chimica (Rome, Italy), 1957 , vol. 47, p. 879,882
反应条件
1: SOCl2 2: aqueous NH3 3: aqueous KBrO View Scheme
参考文献
Angelini
Annali di Chimica (Rome, Italy), 1957 , vol. 47, p. 879,882
反应条件
1: aqueous NH3 2: aqueous KBrO View Scheme
参考文献
Angelini
Annali di Chimica (Rome, Italy), 1957 , vol. 47, p. 879,882
参考文献
Mascarelli; Gatti
Gazzetta Chimica Italiana, 1929 , vol. 59, p. 860
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1929 , vol. <6> 10, p. 442
反应条件
CaO T=400°C; 0.666667 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 41, # 1 p. 1 - 6