N-叔丁基-Alpha-(4-硝基苯基)硝酮合成路线 (共 11 条)
反应条件
3,3-dimethyldioxirane in acetone T=0°C; 0.166667 h;
参考文献
Murray, Robert W.; Singh, Megh
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2954 - 2957
反应条件
urea hydrogen peroxide addition compound; sodium sulfate in methanol T=0 - 20°C;
参考文献
Singh, Bhawan; Jain, Suman L.; Khatri, Praveen K.; Sain, Bir
Green Chemistry, 2009 , vol. 11, # 12 p. 1941 - 1944
反应条件
1: 91 percent / sodium borohydride / methanol / Heating 2: 93 percent / disodium versenate, sodium tungstate, hydrogen peroxide / methanol View Scheme
参考文献
Christensen, Dorthe; Jorgensen, Karl Anker; Hazell, Rita G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2391 - 2397
反应条件
potassium permanganate; tetrabutyl-ammonium chloride in dichloromethane; water 24 h; Ambient temperaturepH 4.1;
参考文献
Christensen, Dorthe; Joergensen, Karl Anker
Journal of Organic Chemistry, 1989 , vol. 54, # 1 p. 126 - 131
参考文献
Emmons
Journal of the American Chemical Society, 1957 , vol. 79, p. 5739,5749
反应条件
2-tert-Butyl-3-phenyloxaziridine T=100°C; P=6000480 Torr; 20 h; Yield given. Yields of byproduct given;
参考文献
Shimizu, Masao; Shibuya, Isao; Taguchi, Yoichi; Hamakawa, Satoshi; Suzuki, Kunio; Hayakawa, Takashi
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 23 p. 3491 - 3492
反应条件
methyl-phenyl-thioether T=100°C; P=6000480 Torr; 20 h; Yield given. Yields of byproduct given;
参考文献
Shimizu, Masao; Shibuya, Isao; Taguchi, Yoichi; Hamakawa, Satoshi; Suzuki, Kunio; Hayakawa, Takashi
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 23 p. 3491 - 3492
反应条件
aluminium trichloride in chloroform-d1 22 h;
参考文献
Christensen, Dorthe; Jorgensen, Karl Anker; Hazell, Rita G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2391 - 2397
反应条件
in deuterated toluene T=95°C; k = 9.8E-6/sec, ΔG* = 30.1 kcal/mol; Product distributionRate constantThermodynamic data;
参考文献
Boyd, Derek R.; Coulter, Peter B.; Hamilton, W. James; Jennings, W. Brian; Wilson, Valerie E.
Tetrahedron Letters, 1984 , vol. 25, # 21 p. 2287 - 2288
参考文献
Boyd, Derek R.; Coulter, Peter B.; McGuckin, M. Rosaleen; Sharma, Narain D.; Jennings, W. Brian; Wilson, Valerie E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 301 - 306