1,3-二甲基-5-[(二甲基氨基)亚甲基]2,4,6-(1H,3H,5H)-三氧代嘧啶合成路线 (共 5 条)
反应条件
in acetonitrile T=20°C; 6 h;
参考文献
Selic, Lovro; Stanovnik, Branko
Tetrahedron, 2001 , vol. 57, # 15 p. 3159 - 3164
反应条件
in diethyl ether T=20°C; 2 h;
参考文献
Obschestvo S Ogranichennoi Otvetstvennostju "Unikorm"; GRANIK, Vladimir Grigorevich; PARSHIN, Valery Aleksandrovich; GOLOVKO, Tatyana Vasilyevna; TUGUSHEVA, Nelya Zarifovna; MEDVEDEVA, Marina Igorevna
Patent: EP2564851 A2, 2013 ;
Location in patent: Paragraph 0014-0015 ;
反应条件
acetic anhydride T=90°C; Condensation; 2 h;
参考文献
Wuerthner, Frank
Synthesis, 1999 , # 12 p. 2103 - 2113
反应条件
in ethyl acetate 0.5 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Kantlehner, Willi; Hauber, Michael
Bulletin des Societes Chimiques Belges, 1994 , vol. 103, # 12 p. 697 - 704
反应条件
acetic acid
T=90 - 100°C; 2 h;
参考文献
Selic, Lovro; Stanovnik, Branko
Tetrahedron, 2001 , vol. 57, # 15 p. 3159 - 3164