2-氨基-5-磺基苯甲酸合成路线 (共 15 条)
反应条件
fuming sulfuric acid; sulfur trioxide T=0 - 180°C; 2 h; Cooling with ice;
参考文献
Harschneck, Tobias; Hummel, Sara; Kirsch, Stefan F.; Klahn, Philipp
Chemistry - A European Journal, 2012 , vol. 18, # 4 p. 1187 - 1193
反应条件
1: With sodium N-bromobenzenesulfonamide; sodium hydroxide; palladium dichloride in water; acetonitrile T=60°C; pH=12; 3.66667 h; 2: in water Acidic conditions;
参考文献
Kumar, C. Vinod; Shivananda; Raju, C. Nagu; Jagadeesh
Synthetic Communications, 2010 , vol. 40, # 23 p. 3480 - 3487
反应条件
sulfuric acid T=180°C;
参考文献
Gazzetta Chimica Italiana, , vol. 63, p. 81,94
反应条件
ammonia T=160 - 180°C;
参考文献
Chemische Berichte, , vol. 24, p. 3805
反应条件
sulfuric acid T=180°C;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , p. 494
反应条件
sulfuric acid Erwaermen des Reaktionsprodukts mit wss. Natriumcarbonat-Loesung;
参考文献
DE499822 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 501
US1887820 , ;
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Journal of the Association of Official Agricultural Chemists, , vol. 38, p. 949,958
反应条件
1: sulfuric acid 2: alcoholic ammonia / 160 - 180 °C View Scheme
参考文献
Chemische Berichte, , vol. 24, p. 3805
反应条件
1: NH2OH+HCl; Na2SO4; H2O / Erwaermen des Reaktionsprodukts mit konz. H2SO4 2: H2O2; aqueous NaOH View Scheme
参考文献
Journal of the Association of Official Agricultural Chemists, , vol. 38, p. 949,958
参考文献
DE307284 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 13, p. 277
DE296941 ;