(-)-1,6-环氧异二氢香芹醇合成路线 （共 6 条）
反应条件
L-Selectridereg; in tetrahydrofuran T=-78°C; 2 h;
参考文献
Nishiyama; Ikeda; Yoshida; Yamamura
Tetrahedron Letters, 1989 , vol. 30, # 1 p. 105 - 108
反应条件
sodium tetrahydroborate in ethanol 24 h; Ambient temperature;
参考文献
Hatakeyama, Susumi; Numata, Hirotoshi; Osanai, Ken; Takano, Seiichi
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3515 - 3517
反应条件
1: 100 percent / H2O2; NaOH / methanol 2: 85 percent / L-Selectride / tetrahydrofuran View Scheme
参考文献
Jones Jr.; Kover
Synthetic Communications, 1995 , vol. 25, # 23 p. 3907 - 3921
反应条件
L-Selectridereg; in tetrahydrofuran T=-70 - -65°C; Reduction;
参考文献
Wang, Jing; Busson, Roger; Blaton, Norbert; Rozenski, Jef; Herdewijn, Piet
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 3051 - 3058
反应条件
1H-imidazole in N,N-dimethyl-formamide
参考文献
Hatakeyama, Susumi; Numata, Hirotoshi; Osanai, Ken; Takano, Seiichi
Journal of Organic Chemistry, 1989 , vol. 54, # 15 p. 3515 - 3517
反应条件
1.1: imidazole
2.1: OsO4, KIO4
2.2: MCPBA
3.1: K2CO3 / methanol
4.1: imidazole
View Scheme
参考文献
Mourino, Antonio; Torneiro, Mercedes; Vitale, Cristian; Fernandez, Sara; Perez-Sestelo, Jose; Anne, Sofia; Gregorio, Carlos
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4713 - 4716
