反应条件
1.1: sodium sulfide; sodium hydrogencarbonate / water; methanol / 25 - 80 °C 2.1: 35 - 40 °C 2.2: 80 - 85 °C 2.3: 25 - 30 °C 3.1: hydrogen / Raney nickel / methanol / 25 - 30 °C / 4654.46 - 5171.62 Torr 4.1: N-ethyl-N,N-diisopropylamine / water / 25 - 95 °C 5.1: thionyl chloride / dichloromethane / 25 - 60 °C 5.2: 55 - 60 °C View Scheme