1,2,2-三氯-1,1-二氟乙烷合成路线 (共 51 条)
参考文献
Zhurnal Obshchei Khimii, , vol. 24, p. 2257,2261; engl. Ausg. S. 2225,2228
反应条件
T=63 - 92°C; durch photochemische Chlorierung;
参考文献
Henne; Ladd
Journal of the American Chemical Society, 1936 , vol. 58, p. 403
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McBee; Bolt
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 412,413
反应条件
aluminium trichloride; water; phosphorus trichoride 1.) 3 h, reflux,; Yield given. Multistep reaction;
参考文献
Bauer, Gert; Haegele, Gerhard; Sartori, Peter
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 95 - 98
反应条件
aluminium trichloride; water; phosphorus trichoride 1.) 1.5 h, reflux; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bauer, Gert; Haegele, Gerhard; Sartori, Peter
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 95 - 98
反应条件
hydrogen fluoride; mercury(II) oxide T=20°C;
参考文献
Henne
Journal of the American Chemical Society, 1938 , vol. 60, p. 1570
参考文献
Henne
Journal of the American Chemical Society, 1938 , vol. 60, p. 1570
反应条件
antimony dichloride trifluoride unter Druck;
参考文献
Henne; Ladd
Journal of the American Chemical Society, 1936 , vol. 58, p. 403
参考文献
McBee; Bolt
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 412,413
参考文献
McBee; Bolt
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 412,413
反应条件
(i) Na, MeOH, (ii) /BRN= 1736764/, DMF; Multistep reaction;
参考文献
Korin'ko,V.A. et al.
Zhurnal Organicheskoi Khimii, 1975 , vol. 11, # 6 p. 1268 - 1274,1254 - 1259