3,4-二甲氧基苯甲酰氯合成路线 （共 99 条）
反应条件
pyridine; thionyl chloride in benzene
参考文献
Kureha Kagaku Kogyo Kabushiki Kaisha
Patent: US4409240 A1, 1983 ;
反应条件
phosphorus pentachloride in diethyl ether T=0°C;
参考文献
Analytical Chemistry, , vol. 53, # 13 p. 1979 - 1982
反应条件
1: KOH / ethanol; H2O / 25 h / Heating 2: SOCl2 / 3 h / Heating View Scheme
参考文献
Molecular Crystals and Liquid Crystals (1969-1991), , vol. 147, p. 1 - 14
反应条件
in dichloromethane T=25°C; Rate constantEquilibrium constant;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 8 p. 1543 - 1551
Zhurnal Organicheskoi Khimii, , vol. 20, # 8 p. 1695 - 1704
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 418
Monatshefte fuer Chemie, , vol. 27, p. 43
参考文献
Chemische Berichte, , vol. 39, p. 4023
反应条件
1: 31 percent / triethylamine / benzene / 2 h / 40 °C / 20 degC, overnight 2: 1. POCl3; 2. 10percent aq. NaOH / 1. dioxane, 80 degC, 4h View Scheme
参考文献
Prizhiyalgovskaya, N. M.; Kon'kov, L. I.; Tarshits, D. L.; Salmina, S. V.; Segizova, N. T.; Suvorov, N. N.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 7 p. 751 - 754
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 7 p. 915 - 918
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola
Acta Chemica Scandinavica, 1997 , vol. 51, # 6-7 p. 718 - 732
反应条件
1: diphenyl phosphoryl azide; triethylamine / 1,4-dioxane / 0.5 h / 20 °C 2: 1,4-dioxane / 2 h / |Reflux View Scheme
参考文献
Sanphanya, Kingkan; Wattanapitayakul, Suvara K.; Phowichit, Suwadee; Fokin, Valery V.; Vajragupta, Opa
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 10 p. 2962 - 2967
