反应条件
in diethyl ether (Ar), stannane added to the Grignard prepared from Mg and C3H7Br in Et2O, refluxed for 3 h; hydrolyzed with satd. NH4Cl soln., diluted with ether, org. layer sepd., washed with water for 3 times, dried over MgSO4, solvent evapd. under reduced pressure;
参考文献
Farah, Dan; Karol, Thomas J.; Kuivila, Henry G.
Organometallics, 1985 , vol. 4, p. 662 - 666
