4,4'-二硫代二苯甲酸二甲酯合成路线 (共 15 条)
参考文献
Young, Robert Norman; Gauthier, Jacques Yves; Coombs, William
Tetrahedron Letters, 1984 , vol. 25, # 17 p. 1753 - 1756
反应条件
sulfuric acid 24 h; Heating;
参考文献
Maxwell, Brendan J.; Tsanaktsidis, John
Journal of the American Chemical Society, 1996 , vol. 118, # 18 p. 4276 - 4283
反应条件
sodium hydrogencarbonate in N,N-dimethyl acetamide 120 h;
参考文献
Marsham, Peter R.; Jackman, Ann L.; Hayter, Anthony J.; Daw, Melanie R.; Snowden, Jayne L.; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2209 - 2218
反应条件
triethylamine in N,N-dimethyl-formamide T=20°C; 3 h;
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 3 p. 207 - 212
反应条件
1: 1.) NaNO2, 2.) Na2S 2: 1.) SOCl2, 2.) Et3N / 1.) reflux, 2 h, 2.) Et2O, reflux, 2 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 61, # 5 p. 1867 - 1869
反应条件
2: 90 percent / aq. KI3 / CHCl3 View Scheme
参考文献
Tetrahedron Letters, , vol. 25, # 17 p. 1753 - 1756
反应条件
1: HCl 2: aq. I2 View Scheme
参考文献
Journal of the Chemical Society, , p. 1947 - 1954
参考文献
Arkiv foer Kemi, , vol. 9, p. 309,310
反应条件
hydrogenchloride; sulfuric acid; zinc 1) glac. HOAc, 100 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 117, # 1 p. 107 - 126
反应条件
in toluene Irradiation; Product distribution;
参考文献
Chemische Berichte, , vol. 117, # 1 p. 107 - 126